Para-fluorination of anilides using electrochemically generated hypervalent iodoarenes
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Abstract
The para-selective fluorination reaction of anilides using electrochemically generated hypervalent ArIF2 is reported, with Et3N ⋅ 5HF serving as fluoride source and as supporting electrolyte. This electrochemical reaction is characterized by a simple set-up, easy scalability and affords a broad variety of fluorinated anilides from easily accessible anilides in good yields up to 86 %.
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Chemistry – a European journal, 28, 41, John Wiley & Sons, Ltd, Weinheim, 2022, https://doi.org/10.1002/chem.202201029