Please use this identifier to cite or link to this item:
http://doi.org/10.25358/openscience-8159
Authors: | Beil, Sebastian B. Pollok, Dennis Waldvogel, Siegfried R. |
Title: | Reproducibility in electroorganic synthesis : myths and misunderstandings |
Online publication date: | 17-Nov-2022 |
Year of first publication: | 2021 |
Language: | english |
Abstract: | The use of electric current as a traceless activator and reagent is experiencing a renaissance. This sustainable synthetic method is evolving into a hot topic in contemporary organic chemistry. Since researchers with various scientific backgrounds are entering this interdisciplinary field, different parameters and methods are reported to describe the experiments. The variation in the reported parameters can lead to problems with the reproducibility of the reported electroorganic syntheses. As an example, parameters such as current density or electrode distance are in some cases more significant than often anticipated. This Minireview provides guidelines on reporting electrosynthetic data and dispels myths about this technique, thereby streamlining the experimental parameters to facilitate reproducibility. |
DDC: | 540 Chemie 540 Chemistry and allied sciences |
Institution: | Johannes Gutenberg-Universität Mainz |
Department: | FB 09 Chemie, Pharmazie u. Geowissensch. |
Place: | Mainz |
ROR: | https://ror.org/023b0x485 |
DOI: | http://doi.org/10.25358/openscience-8159 |
Version: | Published version |
Publication type: | Zeitschriftenaufsatz |
License: | CC BY-NC-ND |
Information on rights of use: | https://creativecommons.org/licenses/by-nc-nd/4.0/ |
Journal: | Angewandte Chemie : International edition 60 27 |
Pages or article number: | 14750 14759 |
Publisher: | Wiley-VCH |
Publisher place: | Weinheim |
Issue date: | 2021 |
ISSN: | 1521-3773 |
Publisher DOI: | 10.1002/anie.202014544 |
Appears in collections: | JGU-Publikationen |
Files in This Item:
File | Description | Size | Format | ||
---|---|---|---|---|---|
reproducibility_in_electroorg-20221021134808442.pdf | 2.67 MB | Adobe PDF | View/Open |