Please use this identifier to cite or link to this item:
http://doi.org/10.25358/openscience-7814
Authors: | Wrobel, Norma Witulski, Bernhard Schollmeyer, Dieter Detert, Heiner |
Title: | 5,11-Dimethyl-6,12-dimethoxyindolo[3,2-b]carbazole |
Online publication date: | 4-Oct-2022 |
Year of first publication: | 2013 |
Language: | english |
Abstract: | The title compound, C(22)H(20)N(2)O(2), was prepared in a twofold Cadogan cyclization followed by double N-methyl-ation. The crystal structure is characterized by a zigzag arrangement of centrosymmetric mol-ecules. The indolocarbazole framework is essentially planar [maximum deviation = 0.028 (2) A] and the meth-oxy groups are orthogonal to this plane [C-C-O-C torsion angle = -88.2 (2) degrees ]. The lengths of the C-N bonds are nearly identical and all C-C bonds of the pyrrole subunit are significantly longer than the C-C bonds in the benzene rings. |
DDC: | 540 Chemie 540 Chemistry and allied sciences |
Institution: | Johannes Gutenberg-Universität Mainz |
Department: | FB 09 Chemie, Pharmazie u. Geowissensch. |
Place: | Mainz |
ROR: | https://ror.org/023b0x485 |
DOI: | http://doi.org/10.25358/openscience-7814 |
Version: | Published version |
Publication type: | Zeitschriftenaufsatz |
License: | CC BY |
Information on rights of use: | https://creativecommons.org/licenses/by/2.0/uk/ |
Journal: | Acta crystallographica : Section E, Structure reports online 69 2 |
Pages or article number: | o255 |
Publisher: | Munksgaard |
Publisher place: | Copenhagen |
Issue date: | 2013 |
ISSN: | 1600-5368 |
Publisher URL: | http://dx.doi.org/10.1107/S1600536813001463 |
Publisher DOI: | 10.1107/S1600536813001463 |
Appears in collections: | DFG-OA-Publizieren (2012 - 2017) |
Files in This Item:
File | Description | Size | Format | ||
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511dimethyl612dimethoxyindolo-20220914001043677.pdf | 276.65 kB | Adobe PDF | View/Open |