Please use this identifier to cite or link to this item:
http://doi.org/10.25358/openscience-6178
Authors: | Kehl, Anton Schupp, Niclas Breising, Valentina M. Schollmeyer, Dieter Waldvogel, Siegfried R. |
Title: | Electrochemical synthesis of carbazoles by dehydrogenative coupling reaction |
Online publication date: | 6-Jul-2021 |
Year of first publication: | 2020 |
Language: | english |
Abstract: | A constant current protocol, employing undivided cells, a remarkably low supporting electrolyte concentration, inexpensive electrode materials, and a straightforward precursor synthesis enabling a novel access to N-protected carbazoles by anodic N,C bond formation using directly generated amidyl radicals is reported. Scalability of the reaction is demonstrated and an easy deblocking of the benzoyl protecting group is presented. |
DDC: | 540 Chemie 540 Chemistry and allied sciences |
Institution: | Johannes Gutenberg-Universität Mainz |
Department: | FB 09 Chemie, Pharmazie u. Geowissensch. |
Place: | Mainz |
ROR: | https://ror.org/023b0x485 |
DOI: | http://doi.org/10.25358/openscience-6178 |
Version: | Published version |
Publication type: | Zeitschriftenaufsatz |
License: | CC BY-NC-ND |
Information on rights of use: | https://creativecommons.org/licenses/by-nc-nd/4.0/ |
Journal: | Chemistry - a European journal 26 68 |
Pages or article number: | 15847 15851 |
Publisher: | Wiley-VCH |
Publisher place: | Weinheim |
Issue date: | 2020 |
ISSN: | 1521-3765 |
Publisher URL: | https://doi.org/10.1002/chem.202003430 |
Publisher DOI: | 10.1002/chem.202003430 |
Appears in collections: | JGU-Publikationen |
Files in This Item:
File | Description | Size | Format | ||
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kehl_anton-electrochemica-20210705132735420.pdf | 964.29 kB | Adobe PDF | View/Open |